By RE approach (to decouple the cathode and anode) combined with voltage profile, overpotential, and polarization curve measurements, the reliability and degradation mechanism of a scaled all-vanadium RFB were investigated, revealing the diverse behaviors of individual. . By RE approach (to decouple the cathode and anode) combined with voltage profile, overpotential, and polarization curve measurements, the reliability and degradation mechanism of a scaled all-vanadium RFB were investigated, revealing the diverse behaviors of individual. . The cathode showed a much higher overpotential than the anode at both the TOC and BOD over 500 cycles. the cathode reaction played a more significant role in limiting the capacity. The cell performance degradation is more contributed by the anode whose overpotential increased gradually upon. . Abstract: As a promising large-scale energy storage technology, all-vanadium redox flow battery has garnered considerable attention. . The all-vanadium flow batteries have gained widespread use in the field of energy storage due to their long lifespan, high efficiency, and safety features. However, in order to further advance their application, it is crucial to uncover the internal energy and mass transfer mechanisms.
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